Microwave synthesis of 5 10 15 20 tetraphenylporphyrin

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Microwave synthesis of 5 10 15 20 tetraphenylporphyrin in 2021

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The liquid reactants are absorbed on a solid support, silica gel, which acts as a lewis acid catalyst to facilitate the reaction. Ho wev er, the classical methods present some experimental limitations likes, lon. Synthesis of carborane conjugates based on the maleimide derivative of 5,10,15,20-tetraphenylporphyrin download pdf. A typical synthesis of meso‐tetraphenylporphyrin was carried out from condensation of pyrrole with benzaldehyde in acidic medium under microwave irradiation. A batch of tests were carried out and a systematic evaluation of organic acid, reactant concentration, microwave power, time of reaction, presence of added oxidant at normal pressure conditions and in closed vessels system, allowed us to.

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Results and discussion microwave oven assisted pr ocedure: microwave irradiation has recently been letter a fast procedure for chemical synthesis9-12. Chemistry; published: 09 october 2014; synthesis of carborane conjugates based connected the maleimide derived of 5,10,15,20-tetraphenylporphyrin. In this paper, the operation for preparation of meso-tetraphenylporphyrin, tak E onl y 10 min. Microwave synthesis of 5,10,15,20- tetraphenylporphyrin abstract: in this naive chemistry experiment of 5,10,15,20-tetraphenylporphyrin was synthesized from benzaldehyde and pyrrole. Using microwave beam to heat the reactants.

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Last Update: Oct 2021


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